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- W2003128454 abstract "Abstract The reaction of the 1,2:3,4-di- O -isopropylidene-6- O -tosyl-α- d -galactopyranose 2 with (11a S )-pyrrolo[2,1- c ][1,4]benzodiazepin-5,11-dione 1 , prepared from l -proline and isatoic anhydride, gave two products which were previously reported as conformational isomers. In this work, an X-ray crystallographic study showed these to be the diastereomeric pair (11a S )- and (11a R )-10- N -(6-deoxy-1,2:3,4-di- O -isopropylidene-α- d -galactopyranos-6-yl)-pyrrolo[2,1- c ][1,4]benzodiazepin-5,11-diones as a consequence of C(11a) epimerization in the benzodiazepine moiety during glycosylation under basic reaction conditions. The hydrosolubility of the deprotected products were compared with those of the analogous benzodiazepine derivatives." @default.
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- W2003128454 date "2001-07-01" @default.
- W2003128454 modified "2023-09-24" @default.
- W2003128454 title "Synthesis and epimerization of 10-N-(6-deoxy-1,2:3,4-di-O-isopropylidene-α-d-galactopyranos-6-yl)-(11aS)-pyrrolo[2,1-c][1,4]benzodiazepin-5,11-dione" @default.
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- W2003128454 doi "https://doi.org/10.1016/s0957-4166(01)00282-8" @default.
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