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- W2003144310 abstract "While the response of the constant current pulsed (CCP) electron-capture detector reflects the extent of reaction between electrons and analyte molecules, it can also be dependent upon other non-analyte electron loss processes. These might include electron losses by reaction with carrier gas impurities, by recombination with positive ions, by diffusion to walls, by ventilation with carrier gas flow, and by migration through small fields generated by contact potentials. These physical factors are examined in detail here with regard to their potential affect on the quantitative response of the CCP electron-capture detector. Experiments indicate that as long as the base frequency of pulsing is moderate to fast, non-analyte electron loss processes within the CCP electron-capture detector will be well-behaved and in harmony with the expectations of simple and idealized theory, and a constant molar response to well-behaved analytes can be expected over the entire dymamic range of the instrument. With the use of slower base frequencies of pulsing, however, non-analyte electron losses are more complicated and non-ideal behavior in the form of non.linear calibration curves is observed. An attempt is made to identify the specific causes of the non-ideal behavior which accompanies the use of the slower pulse frequencies." @default.
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- W2003144310 date "1984-01-01" @default.
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- W2003144310 title "Physical parameters affecting the quantitative response of the constant current electron-capture detector" @default.
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- W2003144310 doi "https://doi.org/10.1016/s0021-9673(01)93705-7" @default.
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