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- W2003151856 abstract "An experiment is presented which allows for the sensitivity-enhanced measurement of proton exchange rates in a HSQC type experiment. Instead of using INEPT type transfer of magnetization from protons to heteronuclei and vice versa, we have used heteronuclear Hartmann-Hahn transfer, which is known to have higher sensitivity in the presence of chemical exchange. Direct NOE's between NH protons and α-protons are suppressed by an exchange-editing step unless the α-resonances are degenerate with the water resonance. A comparison between the exchange-edited HEHAHA-HSQC and a standard exchange-edited HSQC experiment performed on the uniformly15N-labeled staphylococcal nuclease H124L shows an enhancement of approximately 100% with the former experiment. A set of one-dimensional exchange-edited spectra of urea was used for evaluating the ability to extract exchange rates using the presented experiment." @default.
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- W2003151856 title "Sensitivity-Enhanced Detection of Fast Exchanging Protons by an Exchange-Edited Gradient HEHAHA-HSQC Experiment" @default.
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- W2003151856 doi "https://doi.org/10.1006/jmre.1998.1531" @default.
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