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• W2003171911 abstract "In situ x-ray diffraction and Raman spectroscopy were used to explore the pressure-induced phase transformation of spinel ${mathrm{Zn}}_{2}{mathrm{TiO}}_{4}$ to pressures of 52.4 and 81.1 GPa, respectively. Results indicate that spinel ${mathrm{Zn}}_{2}{mathrm{TiO}}_{4}$ initially transforms to the orthorhombic $({mathrm{CaTi}}_{2}{mathrm{O}}_{4})$ structure at 23.7 GPa, and such a phase transition is complete at 32.4 GPa. This high-pressure phase has a bulk modulus of 205 (6) GPa, higher than that of the cubic spinel phase [162 (11) GPa], and at extrapolated to one atmosphere is 2.1% denser than the spinel phase. Upon phase transformation, we observed two additional Raman modes assigned to the newly formed high-pressure phase, whereas the six proceeding Raman modes of the spinel phase disappeared. Upon release of pressure to ambient conditions, the ${mathrm{CaTi}}_{2}{mathrm{O}}_{4}$ phase transforms to a tetragonal polymorph, in which the two observed Raman modes differ in pressure shifts from those of the ${mathrm{CaTi}}_{2}{mathrm{O}}_{4}$ polymorph." @default.
• W2003171911 created "2016-06-24" @default.
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• W2003171911 date "2002-06-26" @default.
• W2003171911 modified "2023-10-10" @default.
• W2003171911 title "<i>In situ</i>x-ray diffraction and Raman spectroscopy of pressure-induced phase transformation in spinel<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant=normal>Zn</mml:mi></mml:mrow><mml:mrow><mml:mn>2</mml:mn></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant=normal>TiO</mml:mi></mml:mrow><mml:mrow><mml:mn>4</mml:mn></mml:mrow></mml:msub></mml:mrow></mml:math>" @default.
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• W2003171911 doi "https://doi.org/10.1103/physrevb.66.024103" @default.
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