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- W2003402902 abstract "Abstract In situ synchrotron time-resolved X-ray diffraction experiments coupled with an infrared imaging camera have been used to reveal the combustion wave structure during the production of MoSi2 by Mechanically Activated Self-propagating High-temperature Synthesis (MASHS). The fast combustion front exhibits a form described as an ‘equilibrium structure’ where the chemical reaction is the sole major driving force. In the MASHS process, oxide-free interfaces between Mo and Si nanocrystallites enhance the reaction Mo+2Si→MoSi2. Exhaustive time-resolved investigations show a possible solid-state process in the first second of the reaction within the combustion front. If preheating is added, the reaction rate is increased, whereas, the presence of α- and β-MoSi2 phases, produced during the ball milling (i.e. mechanical alloying), cause fluctuations in combustion rate. Therefore, an increasing of the mechanical pre-treatment duration leads to an unstable wave by acting directly on the thermal and matter transfer rates." @default.
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- W2003402902 date "2006-01-01" @default.
- W2003402902 modified "2023-10-16" @default.
- W2003402902 title "Combustion wave structure during the MoSi2 synthesis by Mechanically-Activated Self-propagating High-temperature Synthesis (MASHS) : In situ time-resolved investigations." @default.
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- W2003402902 doi "https://doi.org/10.1016/j.intermet.2005.09.001" @default.
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