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• W2003406732 abstract "The crystallization of 5-nitrouracil (5NU) from pure aqueous solution yields two anhydrous polymorphs and a monohydrate depending on the temperature at which the process is carried out. 5NU mimics true polymorphism in that, when retained in aqueous solution, both metastable (anhydrous) forms undergo solvent mediated phase transformations (SMPTs) into the more thermodynamically stable hydrated form as would be predicted by Ostwald’s rule of stages. The phase transformations can occur either in the classical manner of dissolution and recrystallization or, in one case, may in some circumstances be nucleated and morphologically templated by the original crystalline form. There is no appearance from aqueous solution of a known third acentric anhydrous form, previously prepared from acetonitrile solutions. Preliminary experiments suggest this nonappearance may result from the relatively high solubility of this form in aqueous solution." @default.
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• W2003406732 date "2012-09-20" @default.
• W2003406732 modified "2023-10-18" @default.
• W2003406732 title "Polymorphism and Hydrated States in 5-Nitrouracil Crystallized from Aqueous Solution" @default.
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• W2003406732 doi "https://doi.org/10.1021/cg300961m" @default.
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