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- W2003772969 abstract "The unambiguous assignment of the β-hyperfine coupling constants of the radical cations of 5,5″-dimethyl-2,2′ : 5′,2″-terthiophene (11) has been achieved by EPR spectroscopic investigations of the deuteriated compounds 12, 13 and 14. The syntheses of these substances were achieved by cross-coupling following the Negishi and Kumada reaction starting from deuteriated derivatives of chloromethylated thiophene derivatives. The generation of the radical cations was carried out by electrochemical oxidation at a constant potential in the EPR spectrometer. In the presence of acidic compounds a D–H exchange at the β-positions of oligothiophenes was observed. The experimentally determined spin density distribution was rationalized by means of semiempirical quantum mechanical calculations (RHF-INDO-SP). Theoretical and experimental assignments are in good agreement." @default.
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- W2003772969 date "1996-01-01" @default.
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- W2003772969 title "EPR investigations of β-deuteriated 5,5″-dimethyl-2,2′:5′,2″-terthiophenes" @default.
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- W2003772969 doi "https://doi.org/10.1039/p29960002015" @default.
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