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- W2003822956 abstract "Abstract A d -galacto- d -mannan ([α] D +72.0 and d -galactose-to- d -mannose ratio 1:1.14) was isolated from the seeds of Melilotus indica All., syn. M. parviflora Desf. The 1 H- and 13 C-n.m.r., and i.r. spectra indicated the presence of α- d -galactopyranosyl and β- d -mannopyranosyl residues. Methylation of the polysaccharide, followed by hydrolysis, afforded, 2,3,4,6-tetra-, 2,3,6-tri-, 2,3-di-, and 3,4-di- O -methyl- d -mannose, and 2,3,4,6-tetra- and 2,3,6-tri- O -methyl- d -galactose in the molar ratios of 1:2:22:6:27:3. Periodate oxidation of the polysaccharide, followed by reduction and hydrolysis, gave erythritol (1 mol) and glycerol (1.24 mol). Partial acid hydrolysis of the polysaccharide afforded O -β- d -mannopyranosyl-(1→2)- d -mannopyranose, O -β- d -mannopyranosyl-(1→4)- d -mannopyranose, O -α- d -galactopyranosyl-(1→6)- d -mannopyranose, O -α- d -galactopyranosyl-(1→4)- d -galactopyranose, and O -α- d -galactopyranosyl-(1→6)- O -β- d -mannopyranosyl-(1→4)- d -mannopyranose. A highly branched structure having a mannan backbone composed of 36% of (1→4)- and 10% of (1→2)-linked β- d -mannopyranosyl units is proposed for the galactomannan." @default.
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- W2003822956 date "1986-09-01" @default.
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- W2003822956 title "Structure of the d-galacto-d-mannan isolated from the seeds of Melilotus indica All" @default.
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- W2003822956 doi "https://doi.org/10.1016/s0008-6215(00)90196-4" @default.
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