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- W2003994230 abstract "The white crystalline product III from the oxidation of biacetyl bis-benzoylhydrazone, previously believed to be a dibenzoyldihydro-v-tetrazine has now been shown by its N.M.R. and infrared spectrum as well as its ready hydrolysis with acid and the reduction of one benzoyl group to benzyl alcohol to be not a tetrazine but instead the enol benzoate IIIB of 1-benzoylamino-4,5-dimethyl-1,2,3-triazole, an imino anhydride. The previously observed rearrangement of this substance on heating with the formation of 1-[N,N,-dibenzoylamino]-4,5-dimethyl-1,2,3-triazole is then reinterpreted as a 1,3-benzoyl migration from oxygen to nitrogen. Similarly the oxidation product of benzil bis-benzoylhydrazone is, instead of a dihydrotetrazine, the enol benzoate (XII) of 1-benzoylamino-4,5-diphenyl-1,2,3-triazole and the oxidation product from the bis-benzoylhydrazone of pyruvaldehyde is the enol benzoate VIII of 1-benzoylamino-5-methyl-1,2,3-triazole. It seems unlikely that any reported examples of diacyldihydro-v-tetrazines analogous to III are authentic." @default.
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- W2003994230 date "1963-01-01" @default.
- W2003994230 modified "2023-09-23" @default.
- W2003994230 title "Reassignment of structures of the dihydro-v-tetrazines" @default.
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- W2003994230 doi "https://doi.org/10.1016/s0040-4020(01)99243-9" @default.
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