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• W2004013485 abstract "Mesoporous aluminosilicate, FSM-16 (Al-FSM-16(n)), was functionalized by Co-salen modification. The Si/Al ratio, n, was varied from 12.8 to 60.0, and inclusion of Co-salen (N,N′-bis(salicylidene)ethylenediaminocobalt(II)) was carried out by a novel preparative method comprising Co2+ ion exchange in a nonaqueous solution of cobalt(II) acetate and chelation with salen-H2 (N,N′-bis(salicylidene)ethylenediamine). Prominent O2 sorptivity was imparted to this mesoporous material and the amount of O2 sorbed on Co-salen-Al-FSM-16(60.0) was 0.275 mmol g−1 at 298 K, significantly larger than that on Al-FSM-16(60.0) itself (0.085 mmol g−1). The O2 sorption on Co-salen-Al-FSM-16(60.0) remarkably proceeded under a pressure around 20 kPa at 298 K, which was similar to powdery, free Co-salen. The maximum O2/Co-salen ratio for Co-salen included in mesopores was seven times as large as that for neat Co-salen. The pore structure of Al-FSM-16(n) with a high n value was retained through the modification as evidenced by XRD, TEM and N2 adsorption measurements, but that of Al-FSM-16(12.8) was partly collapsed." @default.
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• W2004013485 date "2000-11-01" @default.
• W2004013485 modified "2023-09-29" @default.
• W2004013485 title "Oxygen sorptivity of mesoporous aluminosilicate modified by Co-salen complex" @default.
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• W2004013485 doi "https://doi.org/10.1016/s1387-1811(00)00266-3" @default.
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