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- W2004104026 abstract "Imine ligands terminally bound to triosmium clusters have been prepared by the reaction of Os3(μ-H)2(CO)10 with NH3 and a keto or aldhehydic substrate. However reactions in nonpolar solvents yield only one of the two possible isomers. In contrast, reactions in polar solvents, such as methanol, yield both isomers. Experimental methods are described that clearly demonstrate that the overall stereochemistry of the resulting complexes is dependent upon the competition between intra- and intermolecular hydrogen-bonding interactions. The isomers have been unambiguously assigned using 15N and 13C labeling as well as T1 measurements." @default.
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- W2004104026 date "2000-01-28" @default.
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- W2004104026 title "Coordination of Imines on Os<sub>3</sub> Clusters: Effect of the Solvent in Addressing Isomer Formation" @default.
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- W2004104026 doi "https://doi.org/10.1021/om990754q" @default.
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