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• W2004142724 abstract "Abstract A nanostructured composite powder formed from 75 wt.% NiSb and 25 wt.% Sb was obtained by mechanical alloying binary mixtures of elemental Ni and Sb powders in the composition NiSb 2 for 39 hours. The structural evolution was followed by X-ray diffraction measurements and Rietveld structural refinement. At the end of milling, the crystallites of Sb and NiSb reached a mean size of 17 and 15 nm, respectively. Differential scanning calorimetry measurement showed two exothermic processes at 263 °C and 309 °C. Variable temperature powder X-ray diffraction measurements at 25, 100, 200 and 300 °C showed that the sample is structurally stable until 100 °C. The beginning of the transition NiSb + Sb → NiSb 2 was observed at 200 °C and the nucleation of Sb 2 O 3 was observed at 300 °C in accordance with differential scanning calorimetry measurement. Raman spectroscopy measurements showed neither NiSb nor NiSb 2 compounds produce significant Raman signals when compared with Sb and Sb 2 O 3 ." @default.
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• W2004142724 date "2015-05-12" @default.
• W2004142724 modified "2023-10-16" @default.
• W2004142724 title "Structural, thermal and optical studies of nanocomposite powder NiSb + Sb produced by mechanical alloying" @default.
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• W2004142724 doi "https://doi.org/10.3139/146.111211" @default.
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