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• W2004173853 startingPage "725" @default.
• W2004173853 abstract "An adaptation of the double decomposition method for apatites preparation is tested on lead apatite and applied to the synthesis of lead hydroxyapatite partially potassium substituted. The structure of the sample is carried out by the Rietveld method using powder XRD measurement. The compound crystallizes in the hexagonal system (space group P63/m) with the following cell: a=b=9.8461(3) Å, c=7.3591(3) Å. Final agreement factors Rp, Rwp, RB, and RF are 0.16, 0.11, 0.037, and 0.031, respectively. Results are discussed and compared with those for Pb10(PO4)6(OH)2. According to site occupancy factors, potassium prefers to occupy the site 4f (site(I)). Moreover the structure contains vacancies in both lead and hydroxyl sites. A global mechanism of potassium substitution for lead is proposed." @default.
• W2004173853 created "2016-06-24" @default.
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• W2004173853 date "2000-11-01" @default.
• W2004173853 modified "2023-09-25" @default.
• W2004173853 title "Localization of potassium in substituted lead hydroxyapatite: Pb9.30K0.60(PO4)6(OH)1.20 by X-ray diffraction" @default.
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• W2004173853 doi "https://doi.org/10.1016/s1293-2558(00)01075-x" @default.
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