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- W2004191743 abstract "Selective lipase-catalyzed acylation of 41-desmethoxyrapamycin has been achieved with a quaternary carboxylic acid avoiding the use of vinyl ester activation. Among the acyl donors investigated, the novel butanedione-monooxime and the N-acetylhydroxamate ester proved to be the most efficient donors, comparable in reactivity to the undesired vinyl ester and allowing selective, preparative acylation on gram scale in excellent yields. These new donors are proposed as sustainable and process-friendly alternatives to the widely used vinyl ester substrate activation in lipase-catalyzed acylations of secondary alcohols." @default.
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- W2004191743 date "2010-10-01" @default.
- W2004191743 modified "2023-09-24" @default.
- W2004191743 title "Regioselective lipase-catalyzed acylation of 41-desmethoxy-rapamycin without vinyl esters" @default.
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- W2004191743 doi "https://doi.org/10.1016/j.tetlet.2010.08.020" @default.
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