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• W2004201640 startingPage "121" @default.
• W2004201640 abstract "A relationship between local structure, electrical conductivity (σ) and thermal property of 10SnO2·10P2O5·10Fe2O3·xAgI·(70 − x)V2O5, 10SnO2·10P2O5·10Fe2O3·xAg2O·(70 − x)V2O5 and 10SnO2·10P2O5·10Fe2O3·x/2(AgI·Ag2O)·(70 − x)V2O5 glasses, respectively abbreviated as xAIVSPF, xAOVSPF and xAIAOVSPF with ‘x’ between 0 and 40 mol % were investigated by 57Fe-and 119Sn-Mössbauer spectroscopies, X-ray diffractometry (XRD), Scanning Electron Microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), differential thermal analysis (DTA) and DC two- and four-probe methods. Heat-treatment at 500°C for 100 min of xAIVSPF glass with ‘x’ of 10, 20, 30 and 40 resulted in a marked increase in σ from 2.2 × 10−5, 9.4 × 10−6, 3.2 × 10−6 and 2.6 × 10−6 S cm−1 to 2.6 × 10−1, 2.1 × 10−1, 5.2 × 10−2 and 1.3 × 10−2 S cm−1, respectively. Similar increase in σ caused by heat-treatment was also observed for xAOVSPF and xAIAOVSPF glasses with ‘x’ being equal to or less than 20 mol %. From DTA study, glass transition temperature (Tg) of 248–298°C and crystallization temperature (Tc) of 362–379°C were observed for xAIVSPF glass, whereas gradual decreases in Tg from 277±5 to 216±5°C and Tc from 356±2 to 283±2°C were confirmed for xAOVSPF glass, implying that substitution of AgI for V2O5 didn’t affect the 3D glass network but that of Ag2O causes the cleavage of the 3D glass network. FT-IR study of the heat treated xAOVSPF glass showed the dissappearance of bridging oxygen of P–O–P and V–O–V with the Ag2O content, indicating that cleavage of the 3D glass network caused the decrease of the electrical conductivity. It can be concluded that AgI-subsutituted iron tin phosphovanadate glass is better than Ag2O-subsutituted iron tin phosphovanadate glass for achiving the higher electrical conductivity." @default.
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• W2004201640 date "2015-01-01" @default.
• W2004201640 modified "2023-10-18" @default.
• W2004201640 title "A relationship between electrical conductivity and structural relaxation of 10SnO₂&middot;10Fe₂O₃&middot;10P₂O₅&middot;<i>x</i>AgI&middot;(70 &minus; <i>x</i>)V₂O₅ glass caused by heat-treatment" @default.
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• W2004201640 doi "https://doi.org/10.2109/jcersj2.123.121" @default.
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