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- W2004282144 abstract "A technique has been developed which permits the irradiation of lead alkyls and other unstable compounds with intense 4358-Å mercury light at so low temperatures that photochemical decomposition is negligible. More or less strongly exposed Raman spectra of tetramethyllead, trimethylethyllead, dimethyldiethyllead, methyltriethyllead, tetraethyllead, tetraethyllead-d20 and triethylbismuth, all in the liquid state, were photographed with a three-prism glass spectrograph of reciprocal linear dispersion of 15 Å/mm at 4358 Å. A weakly exposed Raman spectrum of crystalline tetramethyllead was also obtained. To supplement available data, the infrared spectra in the region from 3 to 25 μ were obtained of liquid methyltriethyllead, tetraethyllead, and tetraethyllead-d20, with the aid of a Perkin-Elmer Model 112 double-pass spectrometer. The assignments of vibrational fundamentals for tetramethyllead made by previous workers have been somewhat revised and extended. For the other alkyls, which undoubtedly exist in several conformations, a partial interpretation of the vibrational spectra has been made. Some striking peculiarities of the spectra are pointed out and discussed." @default.
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- W2004282144 date "1964-01-01" @default.
- W2004282144 modified "2023-09-28" @default.
- W2004282144 title "Vibrational spectra of lead alkyls and triethylbismuth" @default.
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- W2004282144 doi "https://doi.org/10.1016/0022-2852(64)90127-4" @default.
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