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- W2004304103 abstract "The crystal structure of a complex formed between BiCl3 and 18-crown-6(1,4,7,10,13,16-hexaoxacyclooctadecane, L) has been determined from X-ray diffractometer data by Patterson and Fourier methods. Crystals are monoclinic, space group Pa, with Z = 2 in a unit cell of dimensions a = 15.09(1), b = 16.60(1), c = 7.987(8) Å, β = 103.0(1)°. The structure, which refined to R = 0.058 for 2766 observed reflections, consists of discrete BiCl3·H2O·L (1) and BiCl3L (2) molecules. In 2 bismuth is sandwiched between two essentially parallel planes containing six oxygens and three chlorines, respectively, and in 1 between three ether and a water oxygen and three chlorines, respectively. In 1 there is intramolecular hydrogen bonding between the water molecule and two of the two ether oxygen atoms not bonded to the metal." @default.
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- W2004304103 date "1990-05-01" @default.
- W2004304103 modified "2023-09-26" @default.
- W2004304103 title "Stereochemical activity of lone pairs. The crystal and molecular structure of a complex of 18-crown-6 (1,4,7,10,13,16-hexaoxacyclooctadecane) with bismuth(III) chloride" @default.
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- W2004304103 doi "https://doi.org/10.1016/s0020-1693(00)84655-1" @default.
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