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- W2004332804 abstract "Deuterated (-)-verapamil, (2S)-(-)-2-(2,5,6-2H3-3,4-dimethoxyphenyl)-2-isopropyl-5-[(2,5,6-2H3-3,4-dimethoxyphenethyl)methylamino]valeronitrile, and its analog (-)-2H5-gallopamil, (2S)-(-)-2-(2,6-2H2-3,4,5-trimethoxyphenyl)-2-isopropyl-5-[(2,5,6-2H3-3,4-dimethoxyphenethyl)methylamino]valeronitrile, were prepared. (-)-Gallopamil readily incorporated five atoms of deuterium into the available positions in the aromatic rings. (-)-2H6-Verapamil was prepared from ring trideuterated 3,4-dimethoxyphenylacetic acid and (2S)-(+)-triphenyl-methoxy-2-[(methanesulfonyl)oxy]propane. Three additional atoms of deuterium were incorporated into the aromatic ring of the N-methyl-3,4-dimethoxyphenethylamine moiety incorporated as the the short N-alkyl side chain. N-13C-Methylverapamil was prepared from N-13C-methyl-3,4-dimethoxyphenethylamine." @default.
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- W2004332804 date "1987-10-01" @default.
- W2004332804 modified "2023-09-23" @default.
- W2004332804 title "Synthesis of deuterated optically active verapamil and gallopamil, and of N-13C-methyl-verapamil" @default.
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- W2004332804 doi "https://doi.org/10.1002/jlcr.2580241007" @default.
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