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• W2004332893 abstract "The novel enantiomeric separation of acidic and neutral compounds by capillary electrochromatography with β-cyclodextrin-bonded positively charged polyacrylamide gels was examined. The columns used are capillaries filled with a positively charged polyacrylamide gel, a so-called monolithic stationary phase, to which allyl carbamoylated β-CD derivatives covalently bind. The capillary wall was activated first by bifunctional reagent to make the resulting gel bind covalently inside the fused-silica tubing. Enantiomeric separations of sixteen acidic and two neutral compounds were achieved using the above-mentioned columns and 200 mmol dm–3 Tris–300 mmol dm–3 boric acid buffer (pH 8.1) as a mobile phase. High efficiencies of up to 150 000 plates m–1 were obtained for dansyl-DL-amino acids. The within-run and between-run reproducibilities of retention time and separation factor were examined for three dansyl-DL-amino acids and warfarin. The relative standard deviations of the within-run and between-run reproducibilities of retention time were less than 1.2 and 1.3% over the six injections, respectively. Those of the separation factor were less than 0.3 and 0.2%, respectively. The gel-filled capillaries were stable for at least four months with intermittent use." @default.
• W2004332893 created "2016-06-24" @default.
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• W2004332893 date "2000-01-01" @default.
• W2004332893 modified "2023-10-10" @default.
• W2004332893 title "Enantiomeric Separations of Acidic and Neutral Compounds by Capillary Electrochromatography with β-Cyclodextrin-Bonded Positively Charged Polyacrylamide Gels" @default.
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• W2004332893 doi "https://doi.org/10.1002/(sici)1521-4168(20000101)23:1<59::aid-jhrc59>3.0.co;2-b" @default.
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