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- W2004354014 abstract "Abstract A well‐defined graft copolymer, polystyrene‐ graft ‐poly(methyl methacrylate), was synthesized in two steps. In the first step, styrene and p ‐vinyl benzene sulfonyl chloride were copolymerized via reversible addition–fragmentation chain transfer polymerization (RAFT) in benzene at 60 °C with 2‐(ethoxycarbonyl)prop‐2‐yl dithiobenzoate as a chain transfer agent and 2,2′‐azobis(isobutyronitrile) as an initiator. In the second step, poly[styrene‐ co ‐ p ‐(vinyl benzene sulfonyl chloride)] was used as a macroinitiator for the atom transfer radical polymerization (ATRP) of methyl methacrylate (MMA) in toluene at 80 °C with CuCl as a catalyst and 2,2′‐bipyridine as a ligand. With sulfonyl chloride groups as the initiating sites for the ATRP of MMA, high initiation efficiencies were obtained. Copyright © 2006 Society of Chemical Industry" @default.
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- W2004354014 date "2005-12-12" @default.
- W2004354014 modified "2023-10-10" @default.
- W2004354014 title "Synthesis of well-defined polystyrene-graft-poly(methyl methacrylate)" @default.
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- W2004354014 doi "https://doi.org/10.1002/pi.1956" @default.
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