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• W2004392313 abstract "Novel one-dimensional heterostructures composed of single crystalline cubic SiC cores, intermediate amorphous SiO2 layers, and single crystalline hexagonal BN (h-BN) sheaths (i.e. SiC–SiO2–BN nanocable) have been successfully fabricated in large scale using SiC–SiO2 nanocables and ammonia borane as starting materials. The structure and chemical composition of the as-synthesized products are determined by powder X-ray diffraction, field emission scanning electron microscopy, high-resolution transmission electron microscopy, X-ray photoelectron spectroscopy, and energy filtered TEM based on electron energy loss spectroscopy. The nanocables are approximately 100 nm in diameter and up to 1 millimetre in length. The intermediate amorphous SiO2 layers and the outer h-BN sheaths are about 10 nm and 5 nm thick, respectively. Interestingly, an increase in the amount of ammonia borane leads to the transformation of SiC–SiO2 nanocables into BN nanotubes. Mass spectrometric analysis shows that the vapors decomposed from ammonia borane play crucial roles both in the growth of the BN sheath on the SiC–SiO2 nanocables and in the transformation to the BN nanotubes. The SiC–SiO2–BN nanocable displays similar photoluminescence (PL) characteristics with respect to the original SiC–SiO2 nanocable but with the 488.5-nm emission peak blue shifting. The synthetic route has also been extended to fabricate SiC–BN nanocables and has proved effective and universal for the synthesis of core–sheath nanostructures with BN sheaths." @default.
• W2004392313 created "2016-06-24" @default.
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• W2004392313 date "2011-01-01" @default.
• W2004392313 modified "2023-09-24" @default.
• W2004392313 title "Novel coaxial SiC–SiO2–BN nanocable: large-scale synthesis, formation mechanism and photoluminescence property" @default.
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• W2004392313 doi "https://doi.org/10.1039/c1jm12008e" @default.
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