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• W2004418675 abstract "Multiwalled carbon nanotubes (MWCNTs) were synthesized by CVD on industrially manufactured highly crystalline vapor-grown carbon fibers (VGCFs). Two catalyst metals (Ni and Fe) and carbon precursor gases (<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msub><mml:mtext>C</mml:mtext><mml:mn>2</mml:mn></mml:msub><mml:msub><mml:mtext>H</mml:mtext><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>and CO) were studied. The catalysts were deposited on the fibers by sputtering and experiments carried out in two different reactors. Samples were characterized by electron microscopy (SEM and TEM). Iron was completely inactive as catalyst with both<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msub><mml:mtext>C</mml:mtext><mml:mn>2</mml:mn></mml:msub><mml:msub><mml:mtext>H</mml:mtext><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>and CO for reasons discussed in the paper. The combination of Ni and<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msub><mml:mtext>C</mml:mtext><mml:mn>2</mml:mn></mml:msub><mml:msub><mml:mtext>H</mml:mtext><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>was very active for secondary CNT synthesis, without any pretreatment of the fibers. The optimal temperature for CNT synthesis was<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msup><mml:mrow><mml:mn>750</mml:mn></mml:mrow><mml:mo>∘</mml:mo></mml:msup><mml:mtext>C</mml:mtext></mml:mrow></mml:math>, with total gas flow of 650 <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msup><mml:mrow><mml:mtext>cm</mml:mtext></mml:mrow><mml:mn>3</mml:mn></mml:msup><mml:msup><mml:mrow><mml:mi>min</mml:mi><mml:mo>⁡</mml:mo></mml:mrow><mml:mrow><mml:mo>−</mml:mo><mml:mn>1</mml:mn></mml:mrow></mml:msup></mml:mrow></mml:math>of<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msub><mml:mtext>C</mml:mtext><mml:mn>2</mml:mn></mml:msub><mml:msub><mml:mtext>H</mml:mtext><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>,<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:msub><mml:mtext>H</mml:mtext><mml:mn>2</mml:mn></mml:msub></mml:mrow></mml:math>, and Ar in 1.0:6.7:30 ratio." @default.
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• W2004418675 date "2008-01-01" @default.
• W2004418675 modified "2023-10-16" @default.
• W2004418675 title "CVD Synthesis of Hierarchical 3D MWCNT/Carbon-Fiber Nanostructures" @default.
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• W2004418675 doi "https://doi.org/10.1155/2008/425195" @default.
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