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• W2004470443 abstract "α,ω-Dicarboxylatopolybutadiene has been prepared and neutralized to varying extents, on either side of stoichiometry, using iron(III) 2-propoxide under anhydrous conditions. These samples have been characterized by extended X-ray absorption fine structure (EXAFS) measurements, and by magnetic measurements and Mössbauer spectroscopy as a function of temperature. It is deduced from EXAFS data, by comparison with iron(III) glycine, that most of the iron is present as μ3-oxo-triion complexes which bond to six polybutadiene chain ends. Static magnetic measurements are consistent with the presence of antiferromagnetic triangular trimers with an S ⋍ 12 ground state. There is some evidence from Mössbauer spectroscopy of the presence of superparamagnetic fine particles with a blocking temperature of at most 7 K, implying the association of some (> 10) of these trimers to give larger clusters." @default.
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• W2004470443 date "1986-07-01" @default.
• W2004470443 modified "2023-10-14" @default.
• W2004470443 title "Microstructure of iron(III) α,ω-dicarboxylatopolybutadiene" @default.
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• W2004470443 doi "https://doi.org/10.1016/0032-3861(86)90060-1" @default.
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