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- W2004501697 abstract "Submicron and micron sized particles containing a crosslinked core and a polar shell were prepared by 3-stage nonaqueous dispersion [NAD] polymerization in an aliphatic hydrocarbon medium. When a poly (12-hydroxystearic acid) [PHS] comb stabilizer was used in all three stages, the particles produced were spherical, submicron in size, and had a relatively broad size distribution. If the monomer mixture in the third stage contained relatively large amounts of butyl acrylate, stable dispersions of sponge-like aggregates, 3–5 μm in size, were obtained. When butyl rubber was employed as a stabilizer precursor in the seed formation step, the shape of the final particles depended upon whether a crosslinker was employed in the second stage polymerization. When a crosslinker was present, the second-stage particles and the subsequent third-stage particles had a shrunken, raisin-like appearance. When no crosslinker was present, spherical particles were obtained. In both cases, the resulting third-stage particles were easily dispersed in water containing a small amount of amine base, indicating that COOH and OH groups are located at the surface (or in a shell at the surface) in these NAD particles. © 1994 John Wiley & Sons, Inc." @default.
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- W2004501697 date "1994-09-01" @default.
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- W2004501697 title "Hydrocarbon dispersions of acrylic microspheres with polar surface functionality" @default.
- W2004501697 doi "https://doi.org/10.1002/pola.1994.080321215" @default.
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