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- W2004609534 abstract "A novel Ag+ ionophore, p-tert-butyl-tetrakis(hydrazinocarbonylmethoxy)thiacalix[4]arene in 1,3-alternate conformation (thiacalix[4]arene tetrahydrazide, 1) was synthesized. Its binding properties towards alkali and transition metal cations were studied by noncompetitive liquid-liquid extraction of alkali metal (Li+, Na+, K+ and Cs+) and transition metal (Co2+, Ni2+, Cu2+, Zn2+, Ag+) picrates. It was found that the thiacalix[4]arene tetrahydrazide exhibited high extractability towards Ag+, lower percent extraction towards Cu2+, and little or no extraction ability towards the others. The selectivity towards Ag+ was further evaluated by competitive Ag+ extraction experiments in the mixture of the above-mentioned nine cations, the concentration of which was monitored with ICP-OES. 1H NMR titration experiments and ESI-MS proved the stoichiometry of 1 to Ag+ was 1:1, and the ′N-Ag+′ interaction with the assistance of thiacalixarene skeleton was primarily involved in the complexation." @default.
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- W2004609534 date "2008-04-01" @default.
- W2004609534 modified "2023-09-25" @default.
- W2004609534 title "An Efficient Ag+ Ionophore Based on Thiacalix[4]arene" @default.
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- W2004609534 doi "https://doi.org/10.1002/cjoc.200890133" @default.
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