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- W2004641354 abstract "Trimethylsilylation followed by recording of 29 Si NMR spectra is a useful method for functional group analysis, especially as the 29 Si lines can be assigned to a particular group by exact experimental techniques. The low sensitivity of these techniques can be overcome by application of reversed methods employing 1 H-detection. Adaptation of heteronuclear multiple quantum coherence 2D NMR spectroscopy to the measurements of 29 Si- 1 H correlations is described, and preparatory experiments for winnowing signals of protons coupled to a 29 Si nucleus are presented. The winnowing experiments designed to optimize 2D experiments have a wider application in identifying the signals of protons that are geminal to the functional group." @default.
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- W2004641354 date "1990-03-01" @default.
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- W2004641354 title "Functional Group Identification by Two-Dimensional <sup>29</sup>Si NMR Spectroscopy with Reversed Detection and Signal Winnowing" @default.
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- W2004641354 doi "https://doi.org/10.1366/0003702904086100" @default.
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