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- W2004649080 abstract "The thermal decompositions of yttrium(III) propionate monohydrate (Y(C2H5CO2)3·H2O) and yttrium(III) butyrate dihydrate (Y(C3H7CO2)3·2H2O) were studied in argon by means of thermogravimetry, differential thermal analysis, IR-spectroscopy, X-ray diffraction and hot-stage microscopy. These two compounds follow a similar decomposition path starting with dehydration, which is complete at 110 °C. The dehydrated salts convert to a dioxycarbonate (Y2O2CO3) via an unstable intermediate product (probably Y2O(C2H5CO2)4 and Y2O(C3H7CO2)4 for the propionate and butyrate respectively), with the evolution of CO2 and a symmetrical ketone consisting of 3-pentanone and 4-heptanone respectively. Final conversion to Y2O3 takes pace with release of CO2. Elemental carbon that is left as a by-product is finally slowly burned by the residual oxygen present in the Ar atmosphere. Fusion is observed at ≈110 °C in anhydrous yttrium butyrate, whereas no melting was evidenced in the propionate." @default.
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- W2004649080 date "2013-05-01" @default.
- W2004649080 modified "2023-10-07" @default.
- W2004649080 title "Thermal decomposition of yttrium(III) propionate and butyrate" @default.
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- W2004649080 doi "https://doi.org/10.1016/j.jaap.2013.01.011" @default.
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