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• W2004690216 abstract "Herein, we describe a study aimed at synthesizing mixed-monolayer-protected CdS nanoparticles and investigating the reactivity of surface-bound functional groups in order to facilitate the immobilization of nanoparticles on a solid substrate as well as the construction of a three-dimensional nanocomposite. CdS nanoparticles initially prepared by the reverse micelle method were used to modify nanoparticle surfaces with 1-decanethiol molecules by ligand exchange. Subsequently, 11-mercapto-1-undecanol was partially incorporated by a place exchange reaction, thereby providing stable, mixed-monolayer-protected CdS nanoparticles. The nanoparticles obtained at each step were characterized by FT-IR and UV−vis spectroscopy, transmission electron microscopy, and elemental analysis. The reactivity of surface hydroxyl groups was verified by a reaction with isocyanate-bearing molecules that provide carbamate bonds in high yields at ambient temperature. The obtained mixed-monolayer-protected nanoparticles were also successfully immobilized on a glass substrate through a carbamate-bond-forming reaction that could be further utilized for multilayer construction in a layer-by-layer fashion." @default.
• W2004690216 created "2016-06-24" @default.
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• W2004690216 date "2004-11-03" @default.
• W2004690216 modified "2023-09-27" @default.
• W2004690216 title "Synthesis, Surface Modification, and Multilayer Construction of Mixed-Monolayer-Protected CdS Nanoparticles" @default.
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• W2004690216 doi "https://doi.org/10.1021/la048729z" @default.
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