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- W2004995181 abstract "[PPh4]2[WSe4] reacts with an equivalent of [Ag(MeCN)4][ClO4] in DMF to afford a linear polymeric cluster {[Ph4P][(μ-WSe4)Ag]}n (1). Treatment of cluster 1 with excess La(NO3)3·3H2O in Me2SO solution resulted in the formation of a helical chain polymeric cluster {[La(Me2SO)8][(μ-WSe4)3Ag3]}n (2). Cluster 2 crystallizes in the monoclinic space group P21/n with four formula units in a cell of dimensions a = 12.7642(5) A, b = 24.1725(9) A, c = 19.4012(7) A, and β = 103.546(11)°. Refinement by full-matrix least-squares techniques gave final residuals R = 0.0540 and Rw = 0.1116 for 494 variables and 7593 reflections (Fo2 > 2.0σ(Fo2)). The anion {[(μ-WSe4)3Ag3]}n3n- in 2 can be described as a butterfly-type SeWSe3Ag2 basic repeating unit linked through interactions with a Ag atom of one fragment and a Ag atom of another to form an intriguing helical array. The CuCN, KCN, and [Et4N]2[WSe4] reaction system resulted in the formation of a novel three-dimensional cluster {[Et4N]2[(μ4-WSe4)Cu4(CN)4]}n (4) either in DM..." @default.
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- W2004995181 date "2010-06-08" @default.
- W2004995181 modified "2023-09-25" @default.
- W2004995181 title "ChemInform Abstract: Heterometallic Polymeric Clusters Containing Tetraselenotungstate Anion: One-Dimensional Helical Chain {[La(Me2SO)8] [(μ-WSe4)3Ag3]}n and Cyanide-Bridged Three-Dimensional Cross-Framework {[Et4N]2 [(μ4-WSe4)Cu4(CN)4] }n." @default.
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- W2004995181 doi "https://doi.org/10.1002/chin.200021024" @default.
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