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• W2005020717 abstract "Abstract A new heterobimetallic, single-source precursor with the formula Ba2(μ-OAc)4(OAc)2Cu4(μ-dmae)4(OH)2 (1) [dmae = N,N-dimethylaminoethanolate and OAc = acetate] has been synthesized by the interaction of Cu(OAc)2 · H2O with Ba(dmae)2 in toluene for the low temperature deposition of CuO–Ba2Cu3O5+x composite thin films. Complex (1) was characterized by melting point, elemental analysis, FT-IR spectroscopy, mass spectrometry, thermal analysis (TGA) and single crystal X-ray diffraction. Complex (1) crystallizes in the triclinic space group P 1 ¯ . A TGA study demonstrated that the complex undergoes controlled thermal decomposition at 400 °C to give the CuO–Ba2Cu3O5+x composite. The chemical composition and surface morphology of the deposited mixed oxide thin films were analyzed by scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX) and X-ray powder diffraction (XRPD), which support the formation of the pure crystalline CuO–Ba2Cu3O5+x composite with particle sizes ranging from 0.08 to 0.4 μm. The thickness and voltage–current characteristics of the thin films were determined with a profilometer and a voltmeter using the four-probe method, respectively." @default.
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• W2005020717 date "2009-03-01" @default.
• W2005020717 modified "2023-10-16" @default.
• W2005020717 title "Low temperature and single-source synthesis of a CuO–Ba2Cu3O5+x composite: Fabrication of thin films and characterization" @default.
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• W2005020717 doi "https://doi.org/10.1016/j.poly.2008.12.041" @default.
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