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- W2005055249 abstract "Abstract In this work, we employed the nonsolvent induced phase separation (NIPS) combined with the gelation method to prepare poly(vinylidene fluoride) (PVDF) membranes. The mixture of N,N-dimethylformamide (DMF) and γ-Butyrolactone (γ-BL) was used as a solvent, and water was used as a nonsolvent. Membrane changed from a cellular to spherulitic morphologies simply by varying the mass ratio of DMF/γ-BL and the PVDF concentration. On quenching the casting solution (with 15 wt% PVDF concentration) in the water bath, the membrane had a uniformly cellular morphology, which resulted from a typical liquid–liquid (L-L) phase separation. At higher PVDF concentrations (≥20 wt%), membranes presented a spherulitic structure, arising from a solid–liquid (S-L) phase separation. The crystallization behavior and crystalline form of the PVDF membrane were identified by different scanning calorimetry (DSC) and Fourier transform infrared spectroscopy (FTIR), respectively. For the 15 wt%-PVDF membrane gained from the mixed solvent with a mass ratio of DMF/γ-BL = 8/2, the highest tensile strength (7.3 MPa) and elongation at break (223%) was obtained." @default.
- W2005055249 created "2016-06-24" @default.
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- W2005055249 date "2015-08-01" @default.
- W2005055249 modified "2023-09-25" @default.
- W2005055249 title "Poly(vinylidene fluoride) membranes prepared via nonsolvent induced phase separation combined with the gelation" @default.
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- W2005055249 doi "https://doi.org/10.1016/j.colsurfa.2015.04.004" @default.
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