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• W2005060946 abstract "A novel MoCuS double cubane-like heterometallic compound, Mo2Cu6S6[SCH2CH2OH]2}(O)2(Ph3P)4, has been obtained from the reaction between {MoCu2S3}(O)(Ph3P)3 and CuSCH2CH2OH in CH2Cl2 solvent. The title complex crystallizes in the monoclinic space group P21/a with cell parameters a = 9.9436(3), b = 30.68(1), c = 15.776(7) Å, β = 104.57(3)°, V = 4658(3) Å 3; Z = 2, dcalc. = 1.43 g cm−3, μ = 18.81 cm−1, T = 296 K, λ(Mo-Kα) = 0.71069 Å, 2θmax = 50°, final R = 0.051 for 3641 observed reflections with I > 5σ(I) and 271 variables. In the complex, two cubane-like fragments are connected by two Cu SCH2CH2OH bonds, in which the SCH2CH2OH− ligand acts as a triple bridge. Three Cu SCH2CH2OH bonds were found to be 2.225(3), 2.405(3) and 2.465(4) Å." @default.
• W2005060946 created "2016-06-24" @default.
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• W2005060946 date "1992-01-01" @default.
• W2005060946 modified "2023-09-27" @default.
• W2005060946 title "Designed synthesis, structure and characterization of a novel double cubane-like molybdenum-copper-sulphur complex, {Mo2Cu6S6[SCH2CH2OH]2}(O)2{Ph3P}4" @default.
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• W2005060946 doi "https://doi.org/10.1016/s0277-5387(00)83569-x" @default.
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