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- W2005232697 abstract "The neutron diffraction powder pattern of UO2 has been recorded at five temperatures between 293 and 1733 K, and the data have been analysed by two methods: the Rietveld profile-refinement procedure and the more conventional approach based on independent integrated intensities. The structural parameters (i.e. the thermal amplitudes of the U and O atoms) derived by the two methods do not differ significantly, but the e.s.d.'s of the parameters given by the Rietveld treatment differ at some temperatures from those obtained by the conventional analysis. These results are discussed in the light of the statistical analysis of the Rietveld procedure published by Sakata & Cooper [J. Appl. Cryst. (1979), 12, 554-563]. At the higher temperatures, the observed mean-square displacements of the U atoms are larger than those calculated by Dolling, Cowley & Woods [Can. J. Phys. (1965), 43, 1397-1413 ] from the analysis of room-temperature phonon dispersion curves." @default.
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- W2005232697 date "1980-03-01" @default.
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- W2005232697 title "Temperature dependence of the atomic thermal displacements in UO<sub>2</sub>: a test case for the Rietveld profile-refinement procedure" @default.
- W2005232697 doi "https://doi.org/10.1107/s0567739480000526" @default.
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