Matches in SemOpenAlex for { <https://semopenalex.org/work/W2005355501> ?p ?o ?g. }
- W2005355501 endingPage "7637" @default.
- W2005355501 startingPage "7630" @default.
- W2005355501 abstract "A dispersive liquid–liquid microextraction (DLLME) method has been optimised for simultaneously extracting 2,4,6-trichloranisole (TCA), 2,3,4,6-tetrachloroanisole (TeCA), 2,4,6-tribromoanisole (TBA), pentachloroanisole (PCA), 2,4,6-trichlorophenol (TCP), 2,3,4,6-tetrachlorophenol (TeCP), 2,4,6-tribromophenol (TBP) and pentachlorophenol (PCP) from wine. The haloanisoles and halophenols were automatically determined using a gas chromatography-electron-capture detection (GC-ECD) system. Derivatisation of halophenols was performed at the same time as DLLME. Firstly, disperser and extraction solvents, salt addition and temperature conditions were selected. Then, the volume of disperser solvent, extraction solvent and derivatisation agent, and the percentage of base were optimised by means of a central composite design combined with desirability functions. The optimal extraction–derivatisation conditions found were 1.3 mL of acetone, 150 μL of carbon tetrachloride, 75 μL of acetic anhydride and a percentage of base of 0.7%; with no salt addition and at room temperature. Under these conditions, the proposed method showed satisfactory linearity (with correlation coefficients over 0.994), repeatability (below 9.7%) and reproducibility (below 9.9%). Moreover, detection limits were lower than the olfactory threshold of the compounds. The developed method was successfully applied to the analysis of red wine samples. To our knowledge, this is the first time that DLLME has been applied to determine cork taint responsible compounds in wine." @default.
- W2005355501 created "2016-06-24" @default.
- W2005355501 creator A5012030254 @default.
- W2005355501 creator A5012649723 @default.
- W2005355501 creator A5017783561 @default.
- W2005355501 creator A5085494620 @default.
- W2005355501 date "2010-12-01" @default.
- W2005355501 modified "2023-10-05" @default.
- W2005355501 title "Optimisation of a dispersive liquid–liquid microextraction method for the simultaneous determination of halophenols and haloanisoles in wines" @default.
- W2005355501 cites W1493185752 @default.
- W2005355501 cites W1534319105 @default.
- W2005355501 cites W1967590475 @default.
- W2005355501 cites W1972596230 @default.
- W2005355501 cites W1977381247 @default.
- W2005355501 cites W1991124498 @default.
- W2005355501 cites W1996508523 @default.
- W2005355501 cites W2001473672 @default.
- W2005355501 cites W2006243227 @default.
- W2005355501 cites W2008133077 @default.
- W2005355501 cites W2018057255 @default.
- W2005355501 cites W2024404830 @default.
- W2005355501 cites W2024491591 @default.
- W2005355501 cites W2029100606 @default.
- W2005355501 cites W2035019470 @default.
- W2005355501 cites W2038021743 @default.
- W2005355501 cites W2038097470 @default.
- W2005355501 cites W2038349874 @default.
- W2005355501 cites W2042455641 @default.
- W2005355501 cites W2045100458 @default.
- W2005355501 cites W2046059756 @default.
- W2005355501 cites W2047345555 @default.
- W2005355501 cites W2047987540 @default.
- W2005355501 cites W2051778893 @default.
- W2005355501 cites W2052991803 @default.
- W2005355501 cites W2056948755 @default.
- W2005355501 cites W2057082331 @default.
- W2005355501 cites W2057873568 @default.
- W2005355501 cites W2057980409 @default.
- W2005355501 cites W2064316402 @default.
- W2005355501 cites W2069751322 @default.
- W2005355501 cites W2069973486 @default.
- W2005355501 cites W2086087976 @default.
- W2005355501 cites W2087588327 @default.
- W2005355501 cites W2091952479 @default.
- W2005355501 cites W2105975384 @default.
- W2005355501 cites W2151710657 @default.
- W2005355501 cites W2162913972 @default.
- W2005355501 cites W2171266592 @default.
- W2005355501 doi "https://doi.org/10.1016/j.chroma.2010.10.032" @default.
- W2005355501 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21035812" @default.
- W2005355501 hasPublicationYear "2010" @default.
- W2005355501 type Work @default.
- W2005355501 sameAs 2005355501 @default.
- W2005355501 citedByCount "48" @default.
- W2005355501 countsByYear W20053555012012 @default.
- W2005355501 countsByYear W20053555012013 @default.
- W2005355501 countsByYear W20053555012014 @default.
- W2005355501 countsByYear W20053555012015 @default.
- W2005355501 countsByYear W20053555012016 @default.
- W2005355501 countsByYear W20053555012017 @default.
- W2005355501 countsByYear W20053555012018 @default.
- W2005355501 countsByYear W20053555012019 @default.
- W2005355501 countsByYear W20053555012020 @default.
- W2005355501 countsByYear W20053555012021 @default.
- W2005355501 countsByYear W20053555012022 @default.
- W2005355501 crossrefType "journal-article" @default.
- W2005355501 hasAuthorship W2005355501A5012030254 @default.
- W2005355501 hasAuthorship W2005355501A5012649723 @default.
- W2005355501 hasAuthorship W2005355501A5017783561 @default.
- W2005355501 hasAuthorship W2005355501A5085494620 @default.
- W2005355501 hasConcept C107872376 @default.
- W2005355501 hasConcept C123460561 @default.
- W2005355501 hasConcept C127413603 @default.
- W2005355501 hasConcept C150077022 @default.
- W2005355501 hasConcept C151304367 @default.
- W2005355501 hasConcept C154020017 @default.
- W2005355501 hasConcept C178790620 @default.
- W2005355501 hasConcept C185592680 @default.
- W2005355501 hasConcept C2775964210 @default.
- W2005355501 hasConcept C2779912340 @default.
- W2005355501 hasConcept C2780471494 @default.
- W2005355501 hasConcept C2781213060 @default.
- W2005355501 hasConcept C31903555 @default.
- W2005355501 hasConcept C42360764 @default.
- W2005355501 hasConcept C43617362 @default.
- W2005355501 hasConcept C4725764 @default.
- W2005355501 hasConcept C55952523 @default.
- W2005355501 hasConcept C92397422 @default.
- W2005355501 hasConceptScore W2005355501C107872376 @default.
- W2005355501 hasConceptScore W2005355501C123460561 @default.
- W2005355501 hasConceptScore W2005355501C127413603 @default.
- W2005355501 hasConceptScore W2005355501C150077022 @default.
- W2005355501 hasConceptScore W2005355501C151304367 @default.
- W2005355501 hasConceptScore W2005355501C154020017 @default.
- W2005355501 hasConceptScore W2005355501C178790620 @default.
- W2005355501 hasConceptScore W2005355501C185592680 @default.
- W2005355501 hasConceptScore W2005355501C2775964210 @default.
- W2005355501 hasConceptScore W2005355501C2779912340 @default.