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• W2005362561 abstract "AEM techniques employing digital filtering, least squares profile fitting, and experimental k-factor calibrations were used to investigate 16 Synroc samples containing simulated Purex (PW-4b-D) HLW at loadings of 10, 15, 19, and 23 wt%. A second group of Synroc samples with 10 wt% HLW also contained additional impurities of F, Na, MgO, P2O5, and Fe2O3. A third set of samples with 10 wt% HLW contained different metal additions of Al, Ni, and Ti, and a sample with no metal addition for comparison. In samples with low Na2O content, it was confirmed that element partitioning is mainly controlled by the ionic radius criterion, with smaller Y, Gd, and U ions having a preference for zirconolite and the larger Ce and Nd ions favoring perovskite. Average relative partitioning coefficients (DZP = metal oxide in zirconolite ÷ wt% metal oxide in perovskite) of 8 samples with 10 wt% HLW and -∼0.5 wt% Na2O are 0.14 ± 0.01, 0.39 ± 0.03, 1.7 ± 0.2, 3.8 ± 1.0, and 2.2 ± 0.8 for Ce, Nd, Gd, Y, and U, respectively. Element partitioning is not strongly affected by additional impurities of F, MgO, P2O5, or Fe2O3; metal addition; or waste loading. Additions of up to ∼3.6 wt% Na2O lead to an increase in the amount of perovskite at the expense of zirconolite as well as a systematic shift in the partitioning of REEs and U from zirconolite into perovskite." @default.
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• W2005362561 date "1995-07-01" @default.
• W2005362561 modified "2023-10-05" @default.
• W2005362561 title "Partitioning of uranium and rare earth elements in synroc: effect of impurities, metal additive, and waste loading" @default.
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• W2005362561 doi "https://doi.org/10.1016/0022-3115(95)00037-2" @default.
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