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- W2005440701 abstract "Abstract ( meso , dl )-3-(Ferrocenylmethyl)pentane-2,4-diol ( 3 ) was synthesized by reduction of 3-(ferrocenylmethyl)pentane-2,4-dione ( 2 ) with LiAlH 4 in a good yield and corresponding monoacetate 4 and diacetate 5 were prepared. Newly prepared compounds are characterized by elemental analysis, IR and NMR spectroscopy and will be used as a substrate or standards for lipase mediated desymmetrization. The structures of 3-(ferrocenylmethyl)pentane-2,4-diol ( 3 ) and 2-(ferrocenylmethyl)propane-1,3-diol diacetate ( 8 ), which is derived from prochiral 2-(ferrocenylmethyl)propane-1,2-diol ( 6 ), were determined by X-ray crystal structure analysis. The conformation of the cyclopentadienyl rings is eclipsed in 3 and almost halfway between eclipsed and staggered in 8 . One O−H⋯O hydrogen bond links the molecules of diol 3 into chains, while one weak C−H⋯π interaction self-assembles the molecules of diacetate 8 into dimers." @default.
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- W2005440701 date "2011-01-01" @default.
- W2005440701 modified "2023-09-26" @default.
- W2005440701 title "Preparation, spectroscopic characterization and crystal structures of ferrocenylalkanediols and derived acetates" @default.
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- W2005440701 doi "https://doi.org/10.1016/j.molstruc.2010.11.040" @default.
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