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- W2005539096 abstract "Abstract It was shown that the reaction of anilines, possessing double bonds in an inside chain (such as N -(2,7-dimethyloctadiene-2,7-yl-1)aniline ( 1a ) and N -prenylaniline ( 1b )) with triethanolamine ( 2 ) in the presence of RuCl 2 (Ph 3 P) 3 involves competition between the reactions of isomerization, hydrogenation of the double bond and heterocyclization. The use of SnCl 2 · 2H 2 O as a co-catalyst promotes the heterocyclization process. It was found that an [Ru]:[Sn] ratio of 1:3 and 1:5 gives the best yield of N -(2,7-dimethyloctadien-2,7-yl-1)indole ( 3a ) and N -prenylindole ( 3b ). Apparently, Ru(II)-Sn(II) complexes containing 3–5 Sn(II) ligands formed in situ are active in heterocyclization of anilines 1a and 1b and suppress isomerization and hydrogenation of the double bond." @default.
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- W2005539096 date "1998-08-01" @default.
- W2005539096 modified "2023-09-27" @default.
- W2005539096 title "Remarkable effect of Sn(II) co-catalyst in the Ru(II) catalyzed heterocyclization of N-terpenyl and N-prenylanilines with triethanolamine" @default.
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- W2005539096 doi "https://doi.org/10.1016/s1387-7003(98)00069-0" @default.
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