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- W2005586255 endingPage "1942" @default.
- W2005586255 startingPage "1934" @default.
- W2005586255 abstract "On treatment with ammonia and benzaldehyde the benzalisoxazolone 3 does not give the aminoketone 7 as assumed by Speroni [1] but a product which has been shown to be identical with the enamine 8 prepared by Ried & Czack [4] from ethyl oximinoacetoacetate and benziminoethyl ether. Authentic aminoketone 7 was synthesized in a three-step procedure starting from the aminonitrile 19. Conversion of 7 into the bromacetyl derivative 23 and subsequent treatment with hexamethylene-tetramine yielded the isoxazolodiazepine 24. Methylation of 24 with diazomethane produced predominantly the N-methyl derivative 1 along with a small amount of the O-methyl compound 25." @default.
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- W2005586255 date "1974-11-06" @default.
- W2005586255 modified "2023-09-25" @default.
- W2005586255 title "Sur l'amino-5-benzoyl-4-méthyl-3-isoxazole: synthèse et transformation en dihydro-6,8-diméthyl-3,8-phényl-4-7H-isoxazolo[5,4-e]diazépin-1,4-one-7" @default.
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- W2005586255 doi "https://doi.org/10.1002/hlca.19740570706" @default.
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