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- W200564156 abstract "The reaction of uranyl nitrate with acetylacetone (HAA) in the presence of ammonia has been re-investigated. Three previous formulations of the product are shown to be incorrect. Microanalysis, conductance measurements, NMR spectra, i.r. spectra and unambiguous synthesis support formulation of the product as the β-ketoamine adduct [UO2(AA)2{OC(CH3)CHC(CH3)NH2}]. Replacement of ammonia by a wide variety of primary and secondary aliphatic amines yields similar β-ketoamine adducts while tertiary amines yield the normal adducts [UO2(AA)2(NR3)]. In contrast to uranyl acetylacetone, uranyl dibenzoylmethanate and uranyl bis(p-methoxybenzoyl)methanate yield only the normal adducts [UO2L2(RNH2)] (L = dibenzoylmethanate or bis(p-methoxybenzoyl) methanate ion) with primary aliphatic amines." @default.
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- W200564156 date "1971-06-01" @default.
- W200564156 modified "2023-09-24" @default.
- W200564156 title "The reaction of ammonia and aliphatic amines with uranyl β-ketoenolates" @default.
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- W200564156 doi "https://doi.org/10.1016/0022-1902(71)80616-4" @default.
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