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- W2005689097 abstract "Barban [4-chlorobut-2-ynyl N-(3-chlorophenyl)carbamate] is analysed as the intact herbicide in wheat products including flour, cereal and bread. Residues of the herbicide are extracted from the samples with methanol. An aliquot of the filtered extract is partitioned between water and dichloromethane. Following this, a Florisil column (3% deactivated) is used for clean-up. The eluted barban is then analyzed directly by liquid chromatography on a LiChrosorb RP-8 column with methanol-water (60:40) as the mobile phase. Recoveries over the range of 0.1–5.0 ppm were generally greater than 80%. Detection limit was estimated to be 0.02 ppm in the samples." @default.
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- W2005689097 date "1980-07-01" @default.
- W2005689097 modified "2023-09-25" @default.
- W2005689097 title "Direct analysis of the herbicide barban in wheat products by reversed-phase liquid chromatography" @default.
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- W2005689097 doi "https://doi.org/10.1016/s0021-9673(00)81548-4" @default.
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