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• W2005702449 abstract "The efficiency of the multicycling procedure for producing thick oxide films on iridium in acid media was observed to decrease with increasing pH, the effect being almost negligible at pH>3.5. By analogy with earlier work on gold this was attributed to increasing inhibition of the rearrangement of the amorphous surface layer with increasing pH due to increased hydroxy complex stability. The mean potential of the maximum of the main charge storage peaks, and that of a further set of minor peaks which appeared only at pH values >2.0, decreased at a rate of about −90 mV per pH unit. Both the hydrogen and oxygen evolution potentials, and the potential maxima of a further set of reversible peaks of high oxidation state transition, exhibited the more conventional (−59 mV per pH unit) behaviour. The variation of the open-circuit rest potential of a cycled iridium electrode with the surface layer in the half-charged state, i.e. [Ir(III)]=[Ir(IV)], varied—depending on the nature of the anion present—from −72 to −77 mV per pH unit. Values significantly closer to the conventional −59 mV per pH unit were observed with a thermally prepared IrO2 layer. These results are compared with recent data by other authors and the role of hydration, and its influence on the acid-base properties of the oxide, are outlined." @default.
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• W2005702449 date "1984-03-01" @default.
• W2005702449 modified "2023-09-27" @default.
• W2005702449 title "Preparation of an oxidized iridium electrode and the variation of its potential with pH" @default.
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• W2005702449 doi "https://doi.org/10.1016/s0022-0728(84)80045-5" @default.
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