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- W2005739596 abstract "A fast and effective method was developed for sequence determination of Cd and Pb in honey by incomplete digestion-high resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GFAAS). Cd and Pb in some honey samples using incomplete digestion treatment were measured by HR-CS GFAAS. The factors influencing determination were investigated by single factor experimental design. The optimal determination conditions were found as follows: NH 4 H 2 PO 4 (10mg/mL) were added as a chemical modifier with the volume of 5μL; pyrolysis temperature 600°C(Cd) and 800°C(Pb); atomization temperature 1100°C(Cd) and 1400°C(Pb). Detection limits (3σ, n =12) were found to be 0.06 μg/L and 0.78 μg/L for Cd and Pb, respectively. The precisions (RSD) for 6 replicate measurements of Cd and Pb in honeys were 3.8% and 2.6%, respectively. Recoveries of added Cd and Pb were varied from 95% to 103%. Therefore, the proposed method was rapid, accurate and stable with a high practical value. It provided scientific basis for multi-element sequence determination in food." @default.
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- W2005739596 date "2014-02-01" @default.
- W2005739596 modified "2023-09-27" @default.
- W2005739596 title "Sequence Determination of Cd and Pb in Honey by Incomplete Digestion-High Resolution Continuum Source Graphite Furnace Atomic Absorption Spectrometry" @default.
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- W2005739596 doi "https://doi.org/10.4028/www.scientific.net/amm.511-512.22" @default.
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