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• W2005763441 abstract "Prior syntheses of porphyrins bearing meso-formyl groups have generally employed the Vilsmeier formylation of an acid-resistant copper or nickel porphyrin. A new approach for the synthesis of free base porphyrins bearing one or two (cis or trans) meso-formyl substituents entails the use of a dipyrromethane bearing an acetal group at the 5-position, a dipyrromethane-1-carbinol bearing an acetal group at the 5-position or carbinol position, or a dipyrromethane-1,9-dicarbinol bearing an acetal group at a carbinol position. Treatment of the resulting meso-acetal-substituted free base porphyrin to gentle acidic hydrolysis yields the corresponding meso-formyl porphyrin." @default.
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• W2005763441 date "2004-06-22" @default.
• W2005763441 modified "2023-10-03" @default.
• W2005763441 title "A New Route to <i>meso</i>-Formyl Porphyrins" @default.
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• W2005763441 doi "https://doi.org/10.1021/jo049819b" @default.
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