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- W2005805344 abstract "Metal complexes, M(l-moba)2(H2O)n (M=Cu(II), n=0; Ni(II), n=2; Pd(II), n=0) and M(bpy)(l-moba)ClO4 (M=Cu(II), Pd(II)), where H(l-moba) denotes 1-l-menthyloxy-3-benzoylacetone, have been synthesized and characterized by means of elemental analyses, NMR spectra, electronic spectra, and circular dichroism spectra. In the NMR spectra of H(l-moba), Pd(l-moba)2, and Pd(bpy)(l-moba)ClO4, the methylene protons adjacent to the l-menthyloxy group were observed as AB quartet. The chloroform solutions of Cu(l-moba)2 and Cu(bpy)(l-moba)ClO4 showed a positive CD band at 15500 and 16200 cm−1, respectively. The chloroform solution of Ni(l-moba)2(H2O)2 also showed a weak, positive CD band near 16000 cm−1. When pyridine or t-butylamine was added to the chloroform solution of Cu(l-moba)2, a negative CD appeared around 17000 cm−1 attributable to the five-coordinate species Cu(l-moba)2B. On the other hand, with adding an amine to the chloroform solution of Ni(l-moba)2(H2O)2, the 16000 cm−1 CD band decreased its intensity and ..." @default.
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- W2005805344 date "1983-06-01" @default.
- W2005805344 modified "2023-10-12" @default.
- W2005805344 title "Noncovalent Interactions in Metal Complexes. VI. Bonding Interaction between Chelate π-System and Menthyl Group in Copper(II), Nickel(II), and Palladium(II) Complexes of 1-<i>l</i>-Menthyloxy-3-benzoylacetone" @default.
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- W2005805344 doi "https://doi.org/10.1246/bcsj.56.1642" @default.
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