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• W2005853165 abstract "The dihydrozirconafuran 3 (2,2-di(cyclopenta-2,4-dien-l-yl)-2,5-dihydro-5,5-dimethyl-3,4-bis(trimethylsilyl)-1,2-oxazirconole) is a valuable synthetic equivalent to the 14-electron fragment Cp2Zr1 Throughout this paper, Cp=η5−C5H5 . The reactions of this metallacycle suppose an equilibrium with an ‘opened’ form [ZrCp2(RCCR)(acetone)], the latter paving the way to numerous ligand replacements. In a solution containing the dihydrozirconafuran and acetone, these reactions are reversible and degenerate, and can be studied by NMR methods: by two-dimensional spectroscopy and by observation of the isotope-induced chemical shifts that occur upon incorporation of (D6)acetone into the metallacycle. The findings give an indirect proof of the described equilibrium." @default.
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• W2005853165 date "1996-03-20" @default.
• W2005853165 modified "2023-10-16" @default.
• W2005853165 title "Ring-Opening Reaction of a Dihydrozirconafuran (= 2,5-Dihydro-1,2-oxazirconole): An equilibrium studied by NMR methods, and its chemical consequences" @default.
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• W2005853165 doi "https://doi.org/10.1002/hlca.19960790213" @default.
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