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- W2006018746 abstract "The crystal and molecular structures of two oxygen-inactive forms of the title complexes, Co(salmedpt), have been determined by X-ray diffractometer data. One form crystallizing from benzene with one molecule of solvent per complex molecule, has the following unit-cell parameters: a = 26.205(5), b = 14.684(3), c = 12.815(3) Å, Z = 8, space group Pcab. Crystals of the other form obtained from acetone are monoclinic with a = 20.842(4), b = 13.842(3), c = 6.795(2), β = 92.58(3) Å, Z = 4, space group P21/a. Both structures have been refined by conventional least-squares techniques to R factors of 0.069 (1177 unique reflections with I > 3σ) and 0.098 (2284 reflections) for the benzene adduct and the form from acetone respectively. The coordination geometry which is identical in both complexes, can be described as a slightly distorted trigonal bipyramid and is essentially similar to that of the deoxy Co(salmaedpt) molecule in the dioxygen adduct [Co(salmedpt)]2·O2·2C6H6." @default.
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- W2006018746 date "1982-01-01" @default.
- W2006018746 modified "2023-09-26" @default.
- W2006018746 title "Crystal and molecular structure of two oxygen-inactive forms of [N,N′-(3,3′-dipropylmethylamine)bis(salicylideneiminato) cobalt(II)]" @default.
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- W2006018746 doi "https://doi.org/10.1016/s0020-1693(00)81919-2" @default.
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