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• W2006106098 abstract "Reactions between [Et4N]2OsCl6 and 1,3-(CH2PBut2)2C6H4 afforded the 16-e chloride complexes OsCl(CO)(PCP) (1) and OsH2Cl(PCP) (2) (PCP = [2,6-(CH2PBut2)2C6H3]-) in methanol/isoamyl alcohol and 2-propanol, respectively. The iodide OsH2I(PCP) (3) was obtained from 2 in methyl iodide. Treatment of 1 and 2 with [BH4]- gave the hydride and dihydrogen compounds OsH(CO)(PCP) (4), OsH(H2)(CO)(PCP) (5), and OsH3(H2)(PCP) (6), while formation of the dihydrogen complexes Os(H2)2Cl(PCP) (7a) and OsH2(H2)Cl(PCP) (7b) was observed by NMR in solution of 2 under H2. The structures of 1, 2, and 3 were determined by X-ray crystallography." @default.
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• W2006106098 date "2001-02-01" @default.
• W2006106098 modified "2023-10-17" @default.
• W2006106098 title "Cyclometalated Osmium Complexes Containing a Tridentate PCP Ligand" @default.
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• W2006106098 doi "https://doi.org/10.1021/om000823x" @default.
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