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- W2006145311 abstract "Vanadium(IV) complexes of formula [V(acRbh)2] with acetylacetone 4-R-benzoylhydrazones (H2acRbh, R=H, Cl, OMe and NO2) have been synthesized and characterized by elemental analysis, IR, UV–vis, and electron paramagnetic resonance (EPR) spectroscopic measurements. All the complexes are one-electron paramagnetic and show very similar axial EPR spectra in frozen solution. In dimethylformamide, the complexes display a V(IV)−V(III) redox couple in the E 1/2 range −0.16–−0.25 V (versus Ag/AgCl). Single crystal X-ray structures of [V(acHbh)2] and [V(acClbh)2] have been determined. The metal center in each complex is in a distorted trigonal prismatic N2O4 coordination sphere assembled by the enolate-O, the imine-N, and the iminolate-O donor acRbh2−." @default.
- W2006145311 created "2016-06-24" @default.
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- W2006145311 date "2012-12-12" @default.
- W2006145311 modified "2023-09-27" @default.
- W2006145311 title "Non-oxo vanadium(IV) complexes with acetylacetone 4-<i>R</i>-benzoylhydrazones" @default.
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- W2006145311 doi "https://doi.org/10.1080/00958972.2012.747089" @default.
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