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- W2006162561 abstract "Reaction of complex salts [(μ-RE)(μ-CO)Fe2(CO)6][HNEt3] (1, E = S, Se) with phosphaalkene t-Bu(Me3SiO)CPSiMe3 (2) has been found to afford a series of new butterfly-shaped Fe2EP clusters of type [(μ-RE)[μ-t-Bu(Me3SiO)CHPH]Fe2(CO)6 (3, RE = EtS; 4, n-PrS; 5, n-BuS; 6, t-BuS; 7, PhSe; 8, p-MeC6H4Se) in quite high yields. This type of cluster may exist as three isomers, namely, e(R)e(H), e(R)a(H), and a(R)a(H), which differ in whether the R group and H atom are attached to E and P atoms with an axial or an equatorial bond. Clusters 3−8 have been characterized by elemental analysis and 1H, 31P, and 77Se NMR spectroscopy, as well as for isomers 3e(R)a(H), 6e(R)a(H), 8e(R)e(H), and 8a(R)a(H) by single-crystal X-ray diffraction analyses. In addition, a possible reaction mechanism has been preliminarily suggested." @default.
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- W2006162561 title "Novel Reaction of Complex Salts [(μ-RE)(μ-CO)Fe<sub>2</sub>(CO)<sub>6</sub>][HNEt<sub>3</sub>] (E = S, Se) with Phosphaalkene t-Bu(Me<sub>3</sub>SiO)CPSiMe<sub>3</sub>. Synthesis and Spectroscopic and Crystallographic Characterization of Butterfly Fe<sub>2</sub>EP Clusters (μ-RE)[μ-t-Bu(Me<sub>3</sub>SiO)CHPH]Fe<sub>2</sub>(CO)<sub>6</sub> (E = S, Se)" @default.
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