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- W2006260996 abstract "The reaction of phosphonium ylides with [PMo12O40]3− consists of successive single electron transfers leading to the formation of the 1e- and 2e-reduced polyoxomolybdates [PMo12O40]4− and [PMo12O40]5−. The ylide is converted into the corresponding phosphonium cation via a radical-cation intermediate. The reaction of phosphanes follows the same pathway but subsequent reactions with residual water produce protons which induce the disproportionation of [PMo12O40]4−. Authentic samples of heteropoly blues in different protonation states have been obtained from the reaction of phenyllithium with [PMo12O40]3− and subsequent protonation with triflic acid. On the basis of electrochemical and spectroscopic data, the reaction product of [PMo12O40]3− with triphenylphosphane, which has been previously described as the oxygen-deficient species [PMo12O39]3−, is reformulated as [H2PMo12O40]3−." @default.
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- W2006260996 date "2000-11-01" @default.
- W2006260996 modified "2023-10-17" @default.
- W2006260996 title "Reduction of the Phosphododecamolybdate Ion by Phosphonium Ylides and Phosphanes" @default.
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- W2006260996 doi "https://doi.org/10.1002/1099-0682(200011)2000:11<2393::aid-ejic2393>3.0.co;2-g" @default.
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